Research Data Leeds Repository

Citation

Halcrow, Malcolm A., Capel Berdiell, Izar, Kulak, Alexander N. and Warriner, Stuart L. (2018) Data to support study of Heterometallic Coordination Polymer Gels Supported by 2,4,6-Tris(Pyrazol-1-yl)-1,3,5-Triazine. University of Leeds. [Dataset] https://doi.org/10.5518/537

Dataset description

Treatment of [M(tpt)2]X2 (M = Fe, Co, Ni; X = BF4, ClO4) with the appropriate silver(I) salt affords thixotropic gels. However, two other related tris-pyrazolyl-azine ligands do not act as gelators under these conditions.

Keywords:	gels; transition metals; N-donor ligands; scanning electron microscopy; X-ray crystallography
Subjects:	F000 - Physical sciences > F100 - Chemistry
Divisions:	Faculty of Engineering and Physical Sciences > School of Chemistry
Related resources:	Location Type https://doi.org/10.1021/acsomega.8b02508 Publication https://eprints.whiterose.ac.uk/140022/ Publication
License:	Creative Commons Attribution 4.0 International (CC BY 4.0)
Date deposited:	18 Dec 2018 12:07
URI:	https://archive.researchdata.leeds.ac.uk/id/eprint/473
Additional details Additional details Creators or authors: Creators ORCID Other ID Email Primary affiliation Primary affiliation ID Primary affiliation ID type Secondary affiliation Secondary affiliation ID Secondary affiliation ID type Halcrow, Malcolm A. https://orcid.org/0000-0001-7491-9034 University of Leeds https://ror.org/024mrxd33 ror Capel Berdiell, Izar https://orcid.org/0000-0003-3828-7097 University of Leeds https://ror.org/024mrxd33 ror Kulak, Alexander N. https://orcid.org/0000-0002-2798-9301 University of Leeds https://ror.org/024mrxd33 ror Warriner, Stuart L. https://orcid.org/0000-0002-7589-6011 University of Leeds https://ror.org/024mrxd33 ror Type of data: Dataset Research funders: Leverhulme Trust Grant numbers: RPG-2015-095 Publication date: 2018 Resource language: English Metadata language: English Research project title: Exploiting a spin-crossover module Publisher: University of Leeds Contact email: m.a.halcrow@leeds.ac.uk Last Modified: 29 Jul 2024 13:20

Files

Documentation

Zip File Manifest [18kB] Zip File Manifest [18kB] Zip File Manifest [18kB] Security: Anyone File name: zip_file_manifest.txt Content type: Documentation Description: Manifest listing contents and file size of zip files Mime-Type: text/plain License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 18kB

compound naming and metadata [709kB] compound naming and metadata [709kB] compound naming and metadata [709kB] Security: Anyone File name: readme.pdf Content type: Documentation Mime-Type: application/pdf License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 709kB

Data

CHN microanalysis [1MB] CHN microanalysis [1MB] CHN microanalysis [1MB] Security: Anyone File name: Microanalysis.pdf Content type: Data Mime-Type: application/pdf License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 1MB

Mass spectrum [433kB] Mass spectrum [433kB] Mass spectrum [433kB] Security: Anyone File name: ESMS.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 433kB

Single crystal X-ray diffraction [1MB] Single crystal X-ray diffraction [1MB] Single crystal X-ray diffraction [1MB] Security: Anyone File name: crystal.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 1MB

X-ray powder diffraction [372kB] X-ray powder diffraction [372kB] X-ray powder diffraction [372kB] Security: Anyone File name: XRPD.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 372kB

NMR spectra [3MB] NMR spectra [3MB] NMR spectra [3MB] Security: Anyone File name: NMR.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 3MB

Scanning electron microscopy [79MB] Scanning electron microscopy [79MB] Scanning electron microscopy [79MB] Security: Anyone File name: SEM.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 79MB

Magnetic susceptibility measurements [199kB] Magnetic susceptibility measurements [199kB] Magnetic susceptibility measurements [199kB] Security: Anyone File name: SQUID.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 199kB

Evans method [23kB] Evans method [23kB] Evans method [23kB] Security: Anyone File name: Evans.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 23kB