Research Data Leeds Repository

Data to support study of Heterometallic Coordination Polymer Gels Supported by 2,4,6-Tris(Pyrazol-1-yl)-1,3,5-Triazine

Citation

Halcrow, Malcolm A. and Capel Berdiell, Izar and Kulak, Alexander N. and Warriner, Stuart L. (2018) Data to support study of Heterometallic Coordination Polymer Gels Supported by 2,4,6-Tris(Pyrazol-1-yl)-1,3,5-Triazine. University of Leeds. [Dataset] https://doi.org/10.5518/537¹

Dataset description

Treatment of [M(tpt)2]X2 (M = Fe, Co, Ni; X = BF4, ClO4) with the appropriate silver(I) salt affords thixotropic gels. However, two other related tris-pyrazolyl-azine ligands do not act as gelators under these conditions.

Keywords:	gels; transition metals; N-donor ligands; scanning electron microscopy; X-ray crystallography
Subjects:	F000 - Physical sciences > F100 - Chemistry2
Divisions:	Faculty of Engineering and Physical Sciences > School of Chemistry3
Related resources:	Location Type https://doi.org/10.1021/acsomega.8b025084 Publication https://eprints.whiterose.ac.uk/140022/5 Publication
License:	Creative Commons Attribution 4.0 International (CC BY 4.0)
Date deposited:	18 Dec 2018 12:07
URI:	https://archive.researchdata.leeds.ac.uk/id/eprint/4736
Additional details Additional details Creators or authors: Creators ORCID Other ID Email Primary affiliation Primary affiliation ID Primary affiliation ID type Secondary affiliation Secondary affiliation ID Secondary affiliation ID type Halcrow, Malcolm A. https://orcid.org/0000-0001-7491-90347 University of Leeds https://ror.org/024mrxd33 ror Capel Berdiell, Izar https://orcid.org/0000-0003-3828-70978 University of Leeds https://ror.org/024mrxd33 ror Kulak, Alexander N. https://orcid.org/0000-0002-2798-93019 University of Leeds https://ror.org/024mrxd33 ror Warriner, Stuart L. https://orcid.org/0000-0002-7589-601110 University of Leeds https://ror.org/024mrxd33 ror Type of data: Dataset Research funders: Leverhulme Trust Grant numbers: RPG-2015-095 Publication date: 2018 Resource language: English Metadata language: English Research project title: Exploiting a spin-crossover module Publisher: University of Leeds Contact email: m.a.halcrow@leeds.ac.uk11 Last Modified: 29 Jul 2024 13:20

Files

Documentation

Zip File Manifest [18kB] 12 Zip File Manifest [18kB] 13 Zip File Manifest [18kB] 14 Security: Anyone File name: zip_file_manifest.txt15 Content type: Documentation Description: Manifest listing contents and file size of zip files Mime-Type: text/plain License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 18kB

compound naming and metadata [709kB] 16 compound naming and metadata [709kB] 17 compound naming and metadata [709kB] 18 Security: Anyone File name: readme.pdf19 Content type: Documentation Mime-Type: application/pdf License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 709kB

Data

CHN microanalysis [1MB] 20 CHN microanalysis [1MB] 21 CHN microanalysis [1MB] 22 Security: Anyone File name: Microanalysis.pdf23 Content type: Data Mime-Type: application/pdf License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 1MB

Mass spectrum [433kB] 24 Mass spectrum [433kB] 25 Mass spectrum [433kB] 26 Security: Anyone File name: ESMS.zip27 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 433kB

Single crystal X-ray diffraction [1MB] 28 Single crystal X-ray diffraction [1MB] 29 Single crystal X-ray diffraction [1MB] 30 Security: Anyone File name: crystal.zip31 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 1MB

X-ray powder diffraction [372kB] 32 X-ray powder diffraction [372kB] 33 X-ray powder diffraction [372kB] 34 Security: Anyone File name: XRPD.zip35 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 372kB

NMR spectra [3MB] 36 NMR spectra [3MB] 37 NMR spectra [3MB] 38 Security: Anyone File name: NMR.zip39 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 3MB

Scanning electron microscopy [79MB] 40 Scanning electron microscopy [79MB] 41 Scanning electron microscopy [79MB] 42 Security: Anyone File name: SEM.zip43 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 79MB

Magnetic susceptibility measurements [199kB] 44 Magnetic susceptibility measurements [199kB] 45 Magnetic susceptibility measurements [199kB] 46 Security: Anyone File name: SQUID.zip47 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 199kB

Evans method [23kB] 48 Evans method [23kB] 49 Evans method [23kB] 50 Security: Anyone File name: Evans.zip51 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 23kB

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