Research Data Leeds Repository

Dataset from Electron Transparent Nanotubes Reveal Crystallization Pathways in Confinement

Galloway, Johanna M and Aslam, Zabeada P and Yeandel, Stephen R and Kulak, Alexander and Ilett, Martha and Kim, Yi-Yeoun and Bejarano-Villafuerte, Angela and Pokroy, Boaz and Drummond-Brydson, Rik M and Freeman, Colin L and Harding, John H and Kapur, Nikil and Meldrum, Fiona C (2023) Dataset from Electron Transparent Nanotubes Reveal Crystallization Pathways in Confinement. University of Leeds. [Dataset] https://doi.org/10.5518/1265

Dataset description

Data includes characterisation of calcium sulfate crystals formed in confinment inside nanopores. Bulk material analysis with powder X-ray diffraction and Raman. Imaging of samples using scanning electron microscopy and transmission electron microscopy. Nanaoscale elemental analyisis using energy dispersive X-ray and nanoscale materials analysis from selected area electron diffraction. These experimental data are supported by molecular dynamics simulations of water approaching and moving within bassanite crystal structures and COMSOL flux modelling of material movement to a crystal forming within a confined pore.

Subjects:	F000 - Physical sciences > F100 - Chemistry > F130 - Structural chemistry > F131 - Crystallography F000 - Physical sciences > F200 - Materials science H000 - Engineering > H100 - General engineering > H160 - Bioengineering, biomedical engineering & clinical engineering > H161 - Biomaterials H000 - Engineering > H100 - General engineering > H160 - Bioengineering, biomedical engineering & clinical engineering > H166 - Imaging J000 - Technologies > J500 - Materials technology not otherwise specified > J510 - Materials technology J000 - Technologies > J500 - Materials technology not otherwise specified > J510 - Materials technology > J511 - Engineering materials
Divisions:	Faculty of Engineering and Physical Sciences > School of Chemistry
Related resources:	Location Type https://doi.org/10.1039/D3SC00869J Publication
License:	Creative Commons Attribution 4.0 International (CC BY 4.0)
Date deposited:	14 Jun 2023 15:03
URI:	http://archive.researchdata.leeds.ac.uk/id/eprint/1122
Additional details Additional details Creators: Creators ORCID Other ID Email Primary affiliation Primary affiliation ID Primary affiliation ID type Secondary affiliation Secondary affiliation ID Secondary affiliation ID type Galloway, Johanna M https://orcid.org/0000-0003-3998-0870 University of Leeds https://ror.org/024mrxd33 ror Aslam, Zabeada P https://orcid.org/0000-0003-3647-8965 University of Leeds https://ror.org/024mrxd33 ror Yeandel, Stephen R https://orcid.org/0000-0002-6977-1677 University of Sheffield https://ror.org/05krs5044 ror Kulak, Alexander https://orcid.org/0000-0002-2798-9301 University of Leeds https://ror.org/024mrxd33 ror Ilett, Martha https://orcid.org/0000-0002-3111-1585 University of Leeds https://ror.org/024mrxd33 ror Kim, Yi-Yeoun https://orcid.org/0000-0002-8503-4554 University of Leeds https://ror.org/024mrxd33 ror Bejarano-Villafuerte, Angela https://orcid.org/0000-0003-4517-3709 University of Leeds https://ror.org/024mrxd33 ror Pokroy, Boaz https://orcid.org/0000-0003-0480-7250 Technion-Israel Institute of Technology https://ror.org/03qryx823 ror Drummond-Brydson, Rik M https://orcid.org/0000-0003-2003-7612 University of Leeds https://ror.org/024mrxd33 ror Freeman, Colin L https://orcid.org/0000-0002-6326-1211 University of Sheffield https://ror.org/05krs5044 ror Rik M Harding, John H https://orcid.org/0000-0001-8429-3151 University of Sheffield https://ror.org/05krs5044 ror Kapur, Nikil https://orcid.org/0000-0003-1041-8390 University of Leeds https://ror.org/024mrxd33 ror Meldrum, Fiona C https://orcid.org/0000-0001-9243-8517 University of Leeds https://ror.org/024mrxd33 ror Type of data: Dataset Research funders: EPSRC, ERC Collection period: Date from Date to 6 April 2018 11 October 2022 Grant numbers: EP/R018820/1, EP/T022108/1, 788968 Publication date: 2023 Resource language: English Research project title: Crystallisation in the Real World, Scientific Computing Research Technology Platform, Dynamin Publisher: University of Leeds Contact Email Address: phyjg@leeds.ac.uk Last Modified: 05 Jul 2023 09:19

Files

Documentation

readme [14kB] readme [14kB] readme [14kB] Visible to: Anyone File name: readme_Galloway-etal_2023.txt Content type: Documentation Mime-Type: text/plain License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 14kB

Data

main_figures.zip [20MB] main_figures.zip [20MB] main_figures.zip [20MB] Visible to: Anyone File name: main_figures.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 20MB

suppl_figures.zip [84MB] suppl_figures.zip [84MB] suppl_figures.zip [84MB] Visible to: Anyone File name: suppl_figures.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 84MB