Research Data Leeds Repository

Dataset from Electron Transparent Nanotubes Reveal Crystallization Pathways in Confinement

Citation

Galloway, Johanna M. and Aslam, Zabeada and Yeandel, Stephen R. and Kulak, Alexander N. and Ilett, Martha and Kim, Yi-Yeoun and Bejarano-Villafuerte, Angela and Pokroy, Boaz and Brydson, Rik and Freeman, Colin L. and Harding, John H. and Kapur, Nikil and Meldrum, Fiona C. (2023) Dataset from Electron Transparent Nanotubes Reveal Crystallization Pathways in Confinement. University of Leeds. [Dataset] https://doi.org/10.5518/1265¹

Dataset description

Data includes characterisation of calcium sulfate crystals formed in confinment inside nanopores. Bulk material analysis with powder X-ray diffraction and Raman. Imaging of samples using scanning electron microscopy and transmission electron microscopy. Nanaoscale elemental analyisis using energy dispersive X-ray and nanoscale materials analysis from selected area electron diffraction. These experimental data are supported by molecular dynamics simulations of water approaching and moving within bassanite crystal structures and COMSOL flux modelling of material movement to a crystal forming within a confined pore.

Subjects:	F000 - Physical sciences > F100 - Chemistry > F130 - Structural chemistry > F131 - Crystallography2 F000 - Physical sciences > F200 - Materials science3 H000 - Engineering > H100 - General engineering > H160 - Bioengineering, biomedical engineering & clinical engineering > H161 - Biomaterials4 H000 - Engineering > H100 - General engineering > H160 - Bioengineering, biomedical engineering & clinical engineering > H166 - Imaging5 J000 - Technologies > J500 - Materials technology not otherwise specified > J510 - Materials technology6 J000 - Technologies > J500 - Materials technology not otherwise specified > J510 - Materials technology > J511 - Engineering materials7
Divisions:	Faculty of Engineering and Physical Sciences > School of Chemistry8
Related resources:	Location Type https://doi.org/10.1039/D3SC00869J9 Publication https://eprints.whiterose.ac.uk/200048/10 Publication
License:	Creative Commons Attribution 4.0 International (CC BY 4.0)
Date deposited:	14 Jun 2023 15:03
URI:	https://archive.researchdata.leeds.ac.uk/id/eprint/112211
Additional details Additional details Creators or authors: Creators ORCID Other ID Email Primary affiliation Primary affiliation ID Primary affiliation ID type Secondary affiliation Secondary affiliation ID Secondary affiliation ID type Galloway, Johanna M. https://orcid.org/0000-0003-3998-087012 University of Leeds https://ror.org/024mrxd33 ror Aslam, Zabeada https://orcid.org/0000-0003-3647-896513 University of Leeds https://ror.org/024mrxd33 ror Yeandel, Stephen R. https://orcid.org/0000-0002-6977-167714 University of Sheffield https://ror.org/05krs5044 ror Kulak, Alexander N. https://orcid.org/0000-0002-2798-930115 University of Leeds https://ror.org/024mrxd33 ror Ilett, Martha https://orcid.org/0000-0002-3111-158516 University of Leeds https://ror.org/024mrxd33 ror Kim, Yi-Yeoun https://orcid.org/0000-0002-8503-455417 University of Leeds https://ror.org/024mrxd33 ror Bejarano-Villafuerte, Angela https://orcid.org/0000-0003-4517-370918 University of Leeds https://ror.org/024mrxd33 ror Pokroy, Boaz https://orcid.org/0000-0003-0480-725019 Technion-Israel Institute of Technology https://ror.org/03qryx823 ror Brydson, Rik https://orcid.org/0000-0003-2003-761220 University of Leeds https://ror.org/024mrxd33 ror Freeman, Colin L. https://orcid.org/0000-0002-6326-121121 University of Sheffield https://ror.org/05krs5044 ror Harding, John H. https://orcid.org/0000-0001-8429-315122 University of Sheffield https://ror.org/05krs5044 ror Kapur, Nikil https://orcid.org/0000-0003-1041-839023 University of Leeds https://ror.org/024mrxd33 ror Meldrum, Fiona C. https://orcid.org/0000-0001-9243-851724 University of Leeds https://ror.org/024mrxd33 ror Type of data: Dataset Research funders: EPSRC, ERC Collection period: Date from Date to 6 April 2018 11 October 2022 Grant numbers: EP/R018820/1, EP/T022108/1, 788968 Publication date: 2023 Resource language: English Metadata language: English Research project title: Crystallisation in the Real World, Scientific Computing Research Technology Platform, Dynamin Publisher: University of Leeds Contact email: phyjg@leeds.ac.uk25 Last Modified: 03 Sep 2024 08:52

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Documentation

readme [14kB] 26 readme [14kB] 27 readme [14kB] 28 Security: Anyone File name: readme_Galloway-etal_2023.txt29 Content type: Documentation Mime-Type: text/plain License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 14kB

Data

main_figures.zip [20MB] 30 main_figures.zip [20MB] 31 main_figures.zip [20MB] 32 Security: Anyone File name: main_figures.zip33 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 20MB

suppl_figures.zip [84MB] 34 suppl_figures.zip [84MB] 35 suppl_figures.zip [84MB] 36 Security: Anyone File name: suppl_figures.zip37 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 84MB

• 1. https://doi.org/10.5518/1265
• 2. https://archive.researchdata.leeds.ac.uk/view/subjects/F131.html
• 3. https://archive.researchdata.leeds.ac.uk/view/subjects/F200.html
• 4. https://archive.researchdata.leeds.ac.uk/view/subjects/H161.html
• 5. https://archive.researchdata.leeds.ac.uk/view/subjects/H166.html
• 6. https://archive.researchdata.leeds.ac.uk/view/subjects/J510.html
• 7. https://archive.researchdata.leeds.ac.uk/view/subjects/J511.html
• 8. https://archive.researchdata.leeds.ac.uk/view/divisions/CHEM/
• 9. https://doi.org/10.1039/D3SC00869J
• 10. https://eprints.whiterose.ac.uk/200048/
• 11. https://archive.researchdata.leeds.ac.uk/id/eprint/1122
• 12. https://orcid.org/0000-0003-3998-0870
• 13. https://orcid.org/0000-0003-3647-8965
• 14. https://orcid.org/0000-0002-6977-1677
• 15. https://orcid.org/0000-0002-2798-9301
• 16. https://orcid.org/0000-0002-3111-1585
• 17. https://orcid.org/0000-0002-8503-4554
• 18. https://orcid.org/0000-0003-4517-3709
• 19. https://orcid.org/0000-0003-0480-7250
• 20. https://orcid.org/0000-0003-2003-7612
• 21. https://orcid.org/0000-0002-6326-1211
• 22. https://orcid.org/0000-0001-8429-3151
• 23. https://orcid.org/0000-0003-1041-8390
• 24. https://orcid.org/0000-0001-9243-8517
• 25. mailto:phyjg@leeds.ac.uk
• 26. https://archive.researchdata.leeds.ac.uk/1122/3/readme_Galloway-etal_2023.txt
• 27. https://archive.researchdata.leeds.ac.uk/1122/3/readme_Galloway-etal_2023.txt
• 28. https://archive.researchdata.leeds.ac.uk/1122/3/readme_Galloway-etal_2023.txt
• 29. https://archive.researchdata.leeds.ac.uk/1122/3/readme_Galloway-etal_2023.txt
• 30. https://archive.researchdata.leeds.ac.uk/1122/1/main_figures.zip
• 31. https://archive.researchdata.leeds.ac.uk/1122/1/main_figures.zip
• 32. https://archive.researchdata.leeds.ac.uk/1122/1/main_figures.zip
• 33. https://archive.researchdata.leeds.ac.uk/1122/1/main_figures.zip
• 34. https://archive.researchdata.leeds.ac.uk/1122/2/suppl_figures.zip
• 35. https://archive.researchdata.leeds.ac.uk/1122/2/suppl_figures.zip
• 36. https://archive.researchdata.leeds.ac.uk/1122/2/suppl_figures.zip
• 37. https://archive.researchdata.leeds.ac.uk/1122/2/suppl_figures.zip