Research Data Leeds Repository

Dataset for ‘Serial Small- and Wide-Angle X-ray Scattering with Laboratory Sources’

Levenstein, Mark A. and Robertson, Karen and Turner, Thomas and Hunter, Liam and O’Brien, Cate and O’Shaughnessy, Cedrick and Kulak, Alexander N. and Le Magueres, Pierre and Wojciechowski, Jakub and Mykhaylyk, Oleksandr O. and Kapur, Nikil and Meldrum, Fiona C. (2022) Dataset for ‘Serial Small- and Wide-Angle X-ray Scattering with Laboratory Sources’. University of Leeds. [Dataset] https://doi.org/10.5518/1170

Dataset description

This dataset contains measurements used in the paper, ‘Serial Small- and Wide-Angle X-ray Scattering with Laboratory Sources' from the journal, IUCrJ (doi: 10.1107/S2052252522007631). Included are the raw SAXS, WAXS, and XRD patterns used in the evaluation of different samples, sample environments, and X-ray scattering instruments. From these data, the authors determined that it is feasible to perform serial SAXS/WAXS analysis of materials using laboratory X-ray sources with the aid of micro- and milli-fluidic sample environments.

Keywords:	Serial crystallography, microfluidics, millifluidics, SAXS/WAXS, powder diffraction
Subjects:	F000 - Physical sciences > F100 - Chemistry > F130 - Structural chemistry > F131 - Crystallography F000 - Physical sciences > F100 - Chemistry > F180 - Analytical chemistry
Divisions:	Faculty of Engineering and Physical Sciences > School of Mechanical Engineering Faculty of Engineering and Physical Sciences > School of Chemistry
Related resources:	Location Type https://doi.org/10.1107/S2052252522007631 Publication https://eprints.whiterose.ac.uk/188957/ Publication
License:	Creative Commons Attribution 4.0 International (CC BY 4.0)
Date deposited:	16 Aug 2022 09:25
URI:	http://archive.researchdata.leeds.ac.uk/id/eprint/1010
Additional details Additional details Creators: Creators ORCID Other ID Email Primary affiliation Primary affiliation ID Primary affiliation ID type Secondary affiliation Secondary affiliation ID Secondary affiliation ID type Levenstein, Mark A. https://orcid.org/0000-0002-2309-3743 CEA, Université Paris Saclay https://ror.org/03xjwb503 ror Robertson, Karen https://orcid.org/0000-0002-0719-5854 University of Nottingham https://ror.org/01ee9ar58 ror Turner, Thomas https://orcid.org/0000-0003-3776-2044 University of Leeds https://ror.org/024mrxd33 ror Hunter, Liam https://orcid.org/0000-0002-2728-0837 University of Leeds https://ror.org/024mrxd33 ror O’Brien, Cate University of Sheffield https://ror.org/05krs5044 ror O’Shaughnessy, Cedrick https://orcid.org/0000-0002-6749-6587 University of Leeds https://ror.org/024mrxd33 ror Kulak, Alexander N. https://orcid.org/0000-0002-2798-9301 University of Leeds https://ror.org/024mrxd33 ror Le Magueres, Pierre Rigaku https://ror.org/01bz6xa25 ror Wojciechowski, Jakub https://orcid.org/0000-0002-4907-3476 Rigaku https://ror.org/01bz6xa25 ror Mykhaylyk, Oleksandr O. https://orcid.org/0000-0003-4110-8328 University of Sheffield https://ror.org/05krs5044 ror Kapur, Nikil https://orcid.org/0000-0003-1041-8390 University of Leeds https://ror.org/024mrxd33 ror Meldrum, Fiona C. https://orcid.org/0000-0001-9243-8517 University of Leeds https://ror.org/024mrxd33 ror Type of data: Dataset Research funders: EPSRC, EPSRC, EPSRC, ERC Grant numbers: EP/T006331/1, EP/R018820/1, EP/M028437/1, 788968 Publication date: 2022 Resource language: English Publisher: University of Leeds Contact Email Address: mark.levenstein@cea.fr Last Modified: 16 Aug 2022 22:35

Files

Documentation

Explanation of data types and content [3kB] Explanation of data types and content [3kB] Explanation of data types and content [3kB] Visible to: Anyone File name: Readme.txt Content type: Documentation Description: Text file Mime-Type: text/plain License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 3kB

Data

SAXS frames [561kB] SAXS frames [561kB] SAXS frames [561kB] Visible to: Anyone File name: SAXS_patterns.zip Content type: Data Description: ZIP folder of EDF files Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 561kB

WAXS frames [7kB] WAXS frames [7kB] WAXS frames [7kB] Visible to: Anyone File name: WAXS_patterns.zip Content type: Data Description: ZIP folder of EDF files Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 7kB

XRD frames of CaCO3 [794MB] XRD frames of CaCO3 [794MB] XRD frames of CaCO3 [794MB] Visible to: Anyone File name: Calcite.zip Content type: Data Description: ZIP folder of binary RODHYPIX files Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 794MB

XRD frames from microfluidics experiment [522kB] XRD frames from microfluidics experiment [522kB] XRD frames from microfluidics experiment [522kB] Visible to: Anyone File name: Microfluidics.zip Content type: Data Description: ZIP folder of binary RODHYPIX files Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 522kB

XRD frames of PCM I [815MB] XRD frames of PCM I [815MB] XRD frames of PCM I [815MB] Visible to: Anyone File name: PCM_I.zip Content type: Data Description: ZIP folder of binary RODHYPIX files Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 815MB