Research Data Leeds Repository

Data to support study of Iron and Silver Complexes of 4-(Imidazol-1-yl)-2,6-di(pyrazol-1-yl)pyridine (L), Including a [Fe3(mu-F)2F6L8]+ Assembly

Citation

Halcrow, Malcolm A. and Capel Berdiell, Izar and Kulmaczewski, Rafał and Warriner, Stuart L. and Cespedes, Oscar (2020) Data to support study of Iron and Silver Complexes of 4-(Imidazol-1-yl)-2,6-di(pyrazol-1-yl)pyridine (L), Including a [Fe3(mu-F)2F6L8]+ Assembly. University of Leeds. [Dataset] https://doi.org/10.5518/895¹

Dataset description

Homoleptic iron and silver complexes of the potentially ditopic title ligand are reported, including an unusual Fe(III)3-fluoro cluster assembly.

Keywords:	iron; silver; N-donor ligands; X-ray crystallography; magnetic measurements
Subjects:	F000 - Physical sciences > F100 - Chemistry2
Divisions:	Faculty of Engineering and Physical Sciences > School of Chemistry3
Related resources:	Location Type https://doi.org/10.1002/ejic.2020007824 Publication https://eprints.whiterose.ac.uk/165412/5 Publication
License:	Creative Commons Attribution 4.0 International (CC BY 4.0)
Date deposited:	11 Sep 2020 14:40
URI:	https://archive.researchdata.leeds.ac.uk/id/eprint/7386
Additional details Additional details Creators or authors: Creators ORCID Other ID Email Primary affiliation Primary affiliation ID Primary affiliation ID type Secondary affiliation Secondary affiliation ID Secondary affiliation ID type Halcrow, Malcolm A. https://orcid.org/0000-0001-7491-90347 University of Leeds https://ror.org/024mrxd33 ror Capel Berdiell, Izar https://orcid.org/0000-0003-3828-70978 University of Leeds https://ror.org/024mrxd33 ror Kulmaczewski, Rafał https://orcid.org/0000-0002-3855-45309 University of Leeds https://ror.org/024mrxd33 ror Warriner, Stuart L. https://orcid.org/0000-0002-7589-601110 University of Leeds https://ror.org/024mrxd33 ror Cespedes, Oscar https://orcid.org/0000-0002-5249-952311 University of Leeds https://ror.org/024mrxd33 ror Type of data: Dataset Research funders: Leverhulme Trust, EPSRC Grant numbers: RPG-2015-095, EP/K012568/1 Publication date: 2020 Resource language: English Metadata language: English Research project title: Exploiting a spin-crossover module, Switchable molecular crystals Publisher: University of Leeds Contact email: m.a.halcrow@leeds.ac.uk12 Last Modified: 31 Oct 2024 12:22

Files

Documentation

compound naming and metadata [218kB] 13 compound naming and metadata [218kB] 14 compound naming and metadata [218kB] 15 Security: Anyone File name: readme.pdf16 Content type: Documentation Mime-Type: application/pdf License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 218kB

Data

Elemental microanayses [176kB] 17 Elemental microanayses [176kB] 18 Elemental microanayses [176kB] 19 Security: Anyone File name: microanalysis.pdf20 Content type: Data Mime-Type: application/pdf License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 176kB

Single crystal X-ray diffraction [15MB] 21 Single crystal X-ray diffraction [15MB] 22 Single crystal X-ray diffraction [15MB] 23 Security: Anyone File name: crystal.zip24 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 15MB

X-ray powder diffraction [248kB] 25 X-ray powder diffraction [248kB] 26 X-ray powder diffraction [248kB] 27 Security: Anyone File name: XRPD.zip28 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 248kB

Nuclear magnetic resonance [5MB] 29 Nuclear magnetic resonance [5MB] 30 Nuclear magnetic resonance [5MB] 31 Security: Anyone File name: NMR.zip32 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 5MB

Magnetic susceptibility measurements [237kB] 33 Magnetic susceptibility measurements [237kB] 34 Magnetic susceptibility measurements [237kB] 35 Security: Anyone File name: SQUID.zip36 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 237kB

Evans method [4MB] 37 Evans method [4MB] 38 Evans method [4MB] 39 Security: Anyone File name: Evans.zip40 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 4MB

Mass spectra [408kB] 41 Mass spectra [408kB] 42 Mass spectra [408kB] 43 Security: Anyone File name: ESMS.zip44 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 408kB

• 1. https://doi.org/10.5518/895
• 2. https://archive.researchdata.leeds.ac.uk/view/subjects/F100.html
• 3. https://archive.researchdata.leeds.ac.uk/view/divisions/CHEM/
• 4. https://doi.org/10.1002/ejic.202000782
• 5. https://eprints.whiterose.ac.uk/165412/
• 6. https://archive.researchdata.leeds.ac.uk/id/eprint/738
• 7. https://orcid.org/0000-0001-7491-9034
• 8. https://orcid.org/0000-0003-3828-7097
• 9. https://orcid.org/0000-0002-3855-4530
• 10. https://orcid.org/0000-0002-7589-6011
• 11. https://orcid.org/0000-0002-5249-9523
• 12. mailto:m.a.halcrow@leeds.ac.uk
• 13. https://archive.researchdata.leeds.ac.uk/738/1/readme.pdf
• 14. https://archive.researchdata.leeds.ac.uk/738/1/readme.pdf
• 15. https://archive.researchdata.leeds.ac.uk/738/1/readme.pdf
• 16. https://archive.researchdata.leeds.ac.uk/738/1/readme.pdf
• 17. https://archive.researchdata.leeds.ac.uk/738/2/microanalysis.pdf
• 18. https://archive.researchdata.leeds.ac.uk/738/2/microanalysis.pdf
• 19. https://archive.researchdata.leeds.ac.uk/738/2/microanalysis.pdf
• 20. https://archive.researchdata.leeds.ac.uk/738/2/microanalysis.pdf
• 21. https://archive.researchdata.leeds.ac.uk/738/3/crystal.zip
• 22. https://archive.researchdata.leeds.ac.uk/738/3/crystal.zip
• 23. https://archive.researchdata.leeds.ac.uk/738/3/crystal.zip
• 24. https://archive.researchdata.leeds.ac.uk/738/3/crystal.zip
• 25. https://archive.researchdata.leeds.ac.uk/738/4/XRPD.zip
• 26. https://archive.researchdata.leeds.ac.uk/738/4/XRPD.zip
• 27. https://archive.researchdata.leeds.ac.uk/738/4/XRPD.zip
• 28. https://archive.researchdata.leeds.ac.uk/738/4/XRPD.zip
• 29. https://archive.researchdata.leeds.ac.uk/738/5/NMR.zip
• 30. https://archive.researchdata.leeds.ac.uk/738/5/NMR.zip
• 31. https://archive.researchdata.leeds.ac.uk/738/5/NMR.zip
• 32. https://archive.researchdata.leeds.ac.uk/738/5/NMR.zip
• 33. https://archive.researchdata.leeds.ac.uk/738/6/SQUID.zip
• 34. https://archive.researchdata.leeds.ac.uk/738/6/SQUID.zip
• 35. https://archive.researchdata.leeds.ac.uk/738/6/SQUID.zip
• 36. https://archive.researchdata.leeds.ac.uk/738/6/SQUID.zip
• 37. https://archive.researchdata.leeds.ac.uk/738/7/Evans.zip
• 38. https://archive.researchdata.leeds.ac.uk/738/7/Evans.zip
• 39. https://archive.researchdata.leeds.ac.uk/738/7/Evans.zip
• 40. https://archive.researchdata.leeds.ac.uk/738/7/Evans.zip
• 41. https://archive.researchdata.leeds.ac.uk/738/8/ESMS.zip
• 42. https://archive.researchdata.leeds.ac.uk/738/8/ESMS.zip
• 43. https://archive.researchdata.leeds.ac.uk/738/8/ESMS.zip
• 44. https://archive.researchdata.leeds.ac.uk/738/8/ESMS.zip