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Data to support study of Iron/2,6-Di(pyrazol-1-yl)pyridine Derivatives with a Discotic Pattern of Alkyl or Alkynyl Substituents
Citation
Halcrow, Malcolm A. and Galadzhun, Iurii and Kulmaczewski, Rafał and Cespedes, Oscar (2021) Data to support study of Iron/2,6-Di(pyrazol-1-yl)pyridine Derivatives with a Discotic Pattern of Alkyl or Alkynyl Substituents. University of Leeds. [Dataset] https://doi.org/10.5518/1001
Dataset description
[Fe(1-bpp)2][BF4]2 derivatives with four long chain alkyl substituents show an irreversible low→high-spin conversion near 350 K, which may reflect melting of the complexes' alkyl substituent conformations
| Keywords: | iron; N-donor ligands; X-ray crystallography; magnetic measurements | ||||||
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| Subjects: | F000 - Physical sciences > F100 - Chemistry | ||||||
| Divisions: | Faculty of Engineering and Physical Sciences > School of Chemistry | ||||||
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| License: | Creative Commons Attribution 4.0 International (CC BY 4.0) | ||||||
| Date deposited: | 11 Jun 2021 12:39 | ||||||
| URI: | https://archive.researchdata.leeds.ac.uk/id/eprint/846 | ||||||
Files
Documentation
Compound naming and metadata [368kB]  |
Compound naming and metadata [368kB] 
Compound naming and metadata [368kB] Data
Elemental microanayses [4MB] |
Single crystal X-ray diffraction [1MB] |
X-ray powder diffraction [505kB] |
Nuclear magnetic resonance [47MB] |
Magnetic susceptibility measurements [1MB] |
Differential scanning calorimetry [5MB] |
Thermogravimetric analysis [1MB] |
Molecular mechanics models [1MB] |