1. ABOUT THE DATASET -------------------- Title: Intensified co-precipitation and ion exchange using an agitated tubular reactor (ATR) for enhanced removal of Cs+ and Sr2+ ions Creator(s): Oguzhan Kivan 1*, Muhammad Yusuf1,2, Rachael Filson-Halliwell1, Jennifer N. Enemmoh1, David Harbottle1, Timothy N. Hunter1* Organisation(s): 1 School of Chemical and Process Engineering, University of Leeds, Leeds, LS2 9JT, U.K. 2 Research Centre for Nuclear Material and Radioactive Waste Technology (PRTBNLR), Research Organization for Nuclear Energy (ORTN), National Research and Innovation Agency (BRIN), South Tangerang, 15314, Indonesia Rights-holder(s):Unless otherwise stated, Copyright 2024 University of Leeds Publication Year: 2024 Description: This is a study for an intensified ion exchange and co-precipitation study combining clinoptilolite and barite. The data was collected from the batch reactor and the agitated tubular reactor and collected samples were centrifuged directly and then was syringe filtered. Supernatant was then checked with atomic adsorption spectrometry to examine the final concentration. Precipitates were dried and characterised by SEM, TEM and BET surface area. Samples collected from the batch and ATR were also studied in Lumireader, Mastersizer and Pressure Filtration Analysis for solid/liquid separation degree. All data were processed in Excel and plotted using OriginPro. Cite as: Kivan, Oguzhan, Filson-Halliwell, Rachael, Enemmoh, Jennifer N.,Hunter, Timothy N. (2024): Intensified co-precipitation and ion exchange using an agitated tubular reactor (ATR) for enhanced removal of Cs+ and Sr2+ ions. University of Leeds. Dataset. https://doi.org/10.5518/1565 Related publication: It is submitted to Chemical Engineering and Processing - Process Intensification. Oguzhan Kivan, Muhammad Yusuf, Rachael Filson-Halliwell, Jennifer N. Enemmoh, David Harbottle, Timothy N. Hunter. Intensified co-precipitation and ion exchange using an agitated tubular reactor (ATR) for enhanced removal of Cs+ and Sr2+ ions, Chemical Engineering and Processing - Process Intensification, 2024 2. TERMS OF USE --------------- Unless otherwise stated, this dataset is licensed under a Creative Commons Attribution 4.0 International Licence: https://creativecommons.org/licenses/by/4.0/.] 3. PROJECT AND FUNDING INFORMATION ---------------------------------- Title: Intensified co-precipitation and ion exchange using an agitated tubular reactor (ATR) for enhanced removal of Cs+ and Sr2+ ions Dates: 2023-2024 Funding organisation: The Engineering and Physical Sciences Research Council (EPSRC) UK Grant no.: grant: EP/V034898/1 4. CONTENTS ----------- File listing ATR Mastersizer - this is a particle size distribution indicating composite flocs synthesised from the batch and the ATR. ATR Removal Efficiency - This is all removal efficiency from ATR and the batch reactor for Cs+ and Sr2+ ions. Lumireader for ATR - This is a sedimentation analysis powered by X-ray showing the sedimentation rates for dispersions from ATR at different agitation frequencies and the batch system. Mastersizer data - This is a originpro file showing how data were plotted. PRESSURE FILTRATON FIXED DATA - This is a further solid/liquid seperation analysis for ATR, batch system as well as pure BaSO4. This data shows the specific cake resistance and the extend of compressibility degree. 1000 ppm Cs - This is a FIB-SEM data showing how deep 1000 ppm of Cs+ ions inetract with the natural clinoptilolite. 1000 ppm Sr - This is a FIB-SEM data showing how deep 1000 ppm of Sr2+ ions inetract with the natural clinoptilolite. 5. METHODS ---------- This is a study for an intensified ion exchange and co-precipitation study combining clinoptilolite and barite. The data was collected from the batch reactor and the agitated tubular reactor and collected samples were centrifuged directly and then was syringe filtered. Supernatant was then checked with atomic adsorption spectrometry to examine the final concentration. Precipitates were dried and characterised by SEM, TEM and BET surface area. Samples collected from the batch and ATR were also studied in Lumireader, Mastersizer and Pressure Filtration Analysis for solid/liquid separation degree. All data were processed in Excel and plotted using OriginPro.