Research Data Leeds Repository

Citation

Hollingsworth, Kristian, McBerney, Ryan, Kaminski, Tomasz P., Balmforth, Matthew R., Tamasanu, Alexandra, Warriner, Stuart L., Webb, Michael E. and Turnbull, W. Bruce (2024) Glycofluoroforms of Lewis-x. University of Leeds. [Dataset] https://doi.org/10.5518/1412

Dataset description

Analytical data of the synthesis of a set of lewis-x glycofluoroforms

Subjects:	F000 - Physical sciences > F100 - Chemistry > F160 - Organic chemistry
Divisions:	Faculty of Engineering and Physical Sciences > School of Chemistry
Related resources:	Location Type https://doi.org/10.1038/S41467-024-51081-7 Publication https://eprints.whiterose.ac.uk/215746/ Publication
License:	Creative Commons Attribution 4.0 International (CC BY 4.0)
Date deposited:	19 Aug 2024 20:05
URI:	https://archive.researchdata.leeds.ac.uk/id/eprint/1316
Additional details Additional details Creators or authors: Creators ORCID Other ID Email Primary affiliation Primary affiliation ID Primary affiliation ID type Secondary affiliation Secondary affiliation ID Secondary affiliation ID type Hollingsworth, Kristian https://orcid.org/0000-0003-3163-7111 University of Leeds https://ror.org/024mrxd33 ror McBerney, Ryan https://orcid.org/0000-0002-4631-0800 University of Leeds https://ror.org/024mrxd33 ror Kaminski, Tomasz P. https://orcid.org/0000-0003-4823-3797 University of Leeds https://ror.org/024mrxd33 ror Balmforth, Matthew R. https://orcid.org/0000-0003-2651-9428 University of Leeds https://ror.org/024mrxd33 ror Tamasanu, Alexandra https://orcid.org/0009-0007-5253-242X University of Leeds https://ror.org/024mrxd33 ror Warriner, Stuart L. https://orcid.org/0000-0002-7589-6011 University of Leeds https://ror.org/024mrxd33 ror Webb, Michael E. https://orcid.org/0000-0003-3574-4686 University of Leeds https://ror.org/024mrxd33 ror Turnbull, W. Bruce https://orcid.org/0000-0002-7352-0360 University of Leeds https://ror.org/024mrxd33 ror Type of data: Dataset Research funders: BBSRC, EPSRC, Wellcome Trust Grant numbers: BB/M028747/1 Publication date: 2024 Resource language: English Metadata language: English Publisher: University of Leeds Contact email: w.b.turnbull@leeds.ac.uk Last Modified: 03 Dec 2024 12:29

Files

Data

SI 1.1 NMR spectra of ITag synthesis [863kB] SI 1.1 NMR spectra of ITag synthesis [863kB] SI 1.1 NMR spectra of ITag synthesis [863kB] Security: Anyone File name: SI_1.1_NMR_spectra_of_Itag_synthesis.zip Content type: Data Description: Bruker FID data and associated files for the 1H, 13C spectra for 1.1.2 1-Methyl-3-((4-[(prop-2-yn-1-yl)carbamoyl]phenyl)methyl)imidazol-1-ium Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 863kB

SI 1.2 HRMS spectra of LewisX synthesis [609MB] SI 1.2 HRMS spectra of LewisX synthesis [609MB] SI 1.2 HRMS spectra of LewisX synthesis [609MB] Security: Anyone File name: SI_1.2_HRMS_spectra_of_LewisX_synthesis.zip Content type: Data Description: Bruker electrospray mass spectra data files for LeX1 to LeX24 Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 609MB

SI 2.11 Isothermal Titration Calorimetry of (a) Classical and (b) El Tor CTB with LewisX [170kB] SI 2.11 Isothermal Titration Calorimetry of (a) Classical and (b) El Tor CTB with LewisX [170kB] SI 2.11 Isothermal Titration Calorimetry of (a) Classical and (b) El Tor CTB with LewisX [170kB] Security: Anyone File name: SI_2.11_Isothermal_Titration_Calorimetry_of_a_Classical_and_b_El_Tor_CTB_with_LewisX.zip Content type: Data Description: MicroCal isothermal titration calorimetry .itc text files for titration and control ligand-into-buffer control Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 170kB

SI 2.18 HRMS ITag screening assay mass spectra of both LacNAc and Lewis X synthesis [4GB] SI 2.18 HRMS ITag screening assay mass spectra of both LacNAc and Lewis X synthesis [4GB] SI 2.18 HRMS ITag screening assay mass spectra of both LacNAc and Lewis X synthesis [4GB] Security: Anyone File name: SI_2.18_HRMS_ITag_screening_assay_mass_spectra_of_both_LacNAc_and_Lewis_X_synthesis.zip Content type: Data Description: Bruker electrospray mass spectra data files Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 4GB

SI 2.19 NMR spectra of the upscaled LewisX and its glycofluoroforms [253MB] SI 2.19 NMR spectra of the upscaled LewisX and its glycofluoroforms [253MB] SI 2.19 NMR spectra of the upscaled LewisX and its glycofluoroforms [253MB] Security: Anyone File name: SI_2.19_NMR_spectra_of_the_upscaled_LewisX_and_its_glycofluoroforms.zip Content type: Data Description: Bruker FID data and associated files for the 1H, 13C, 19F, 19F{1H}, COSY, HSBC and HSQC spectra for LeX1 to LeX24 Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 253MB