Research Data Leeds Repository

Data to support study of silver(I) complexes of bis- and tris-(pyrazolyl)azine derivatives – dimers, coordination polymers and a pentametallic assembly

Citation

Halcrow, Malcolm A. and Capel Berdiell, Izar and Warriner, Stuart L. (2018) Data to support study of silver(I) complexes of bis- and tris-(pyrazolyl)azine derivatives – dimers, coordination polymers and a pentametallic assembly. University of Leeds. [Dataset] https://doi.org/10.5518/346¹

Dataset description

Two solvatomorphs of [Ag(tpt)]BF4·nMeNO2 (tpt = 2,4,6-tri{pyrazol-1-yl}pyridine) form face-to-face dimers linked by bridging pyrazolyl donors, or an unsupported chain-of-helicate dimers. Discrete silver dimers, coordination polymers and a pentanuclear cluster supported by related heterocyclic ligands are also described

Keywords:	silver; N-donor ligands; coordination polymers; X-ray crystallography
Subjects:	F000 - Physical sciences > F100 - Chemistry2
Divisions:	Faculty of Engineering and Physical Sciences > School of Chemistry3
Related resources:	Location Type https://doi.org/10.1039/C8DT00640G4 Publication https://eprints.whiterose.ac.uk/129258/5 Publication
License:	Creative Commons Attribution 4.0 International (CC BY 4.0)
Date deposited:	16 Mar 2018 11:46
URI:	https://archive.researchdata.leeds.ac.uk/id/eprint/3306
Additional details Additional details Creators or authors: Creators ORCID Other ID Email Primary affiliation Primary affiliation ID Primary affiliation ID type Secondary affiliation Secondary affiliation ID Secondary affiliation ID type Halcrow, Malcolm A. https://orcid.org/0000-0001-7491-90347 University of Leeds https://ror.org/024mrxd33 ror Capel Berdiell, Izar https://orcid.org/0000-0003-3828-70978 University of Leeds https://ror.org/024mrxd33 ror Warriner, Stuart L. https://orcid.org/0000-0002-7589-60119 University of Leeds https://ror.org/024mrxd33 ror Type of data: Dataset Research funders: Leverhulme Trust Grant numbers: RPG-2015-095 Publication date: 2018 Resource language: English Metadata language: English Research project title: Exploiting a spin-crossover module Publisher: University of Leeds Contact email: m.a.halcrow@leeds.ac.uk10 Last Modified: 08 Aug 2024 10:54

Files

Documentation

compound naming and metadata [300kB] 11 compound naming and metadata [300kB] 12 compound naming and metadata [300kB] 13 Security: Anyone File name: readme.pdf14 Content type: Documentation Mime-Type: application/pdf License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 300kB

Data

CHN microanalysis [2MB] 15 CHN microanalysis [2MB] 16 CHN microanalysis [2MB] 17 Security: Anyone File name: Microanalyses.pdf18 Content type: Data Mime-Type: application/pdf License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 2MB

Mass spectrum [878kB] 19 Mass spectrum [878kB] 20 Mass spectrum [878kB] 21 Security: Anyone File name: ESMS.zip22 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 878kB

Single crystal X-ray diffraction [2MB] 23 Single crystal X-ray diffraction [2MB] 24 Single crystal X-ray diffraction [2MB] 25 Security: Anyone File name: crystal.zip26 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 2MB

X-ray powder diffraction [431kB] 27 X-ray powder diffraction [431kB] 28 X-ray powder diffraction [431kB] 29 Security: Anyone File name: XRPD.zip30 Content type: Data Mime-Type: XRPD.zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 431kB

NMR spectra [1MB] 31 NMR spectra [1MB] 32 NMR spectra [1MB] 33 Security: Anyone File name: NMR.zip34 Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 1MB

• 1. https://doi.org/10.5518/346
• 2. https://archive.researchdata.leeds.ac.uk/view/subjects/F100.html
• 3. https://archive.researchdata.leeds.ac.uk/view/divisions/CHEM/
• 4. https://doi.org/10.1039/C8DT00640G
• 5. https://eprints.whiterose.ac.uk/129258/
• 6. https://archive.researchdata.leeds.ac.uk/id/eprint/330
• 7. https://orcid.org/0000-0001-7491-9034
• 8. https://orcid.org/0000-0003-3828-7097
• 9. https://orcid.org/0000-0002-7589-6011
• 10. mailto:m.a.halcrow@leeds.ac.uk
• 11. https://archive.researchdata.leeds.ac.uk/330/1/readme.pdf
• 12. https://archive.researchdata.leeds.ac.uk/330/1/readme.pdf
• 13. https://archive.researchdata.leeds.ac.uk/330/1/readme.pdf
• 14. https://archive.researchdata.leeds.ac.uk/330/1/readme.pdf
• 15. https://archive.researchdata.leeds.ac.uk/330/2/Microanalyses.pdf
• 16. https://archive.researchdata.leeds.ac.uk/330/2/Microanalyses.pdf
• 17. https://archive.researchdata.leeds.ac.uk/330/2/Microanalyses.pdf
• 18. https://archive.researchdata.leeds.ac.uk/330/2/Microanalyses.pdf
• 19. https://archive.researchdata.leeds.ac.uk/330/3/ESMS.zip
• 20. https://archive.researchdata.leeds.ac.uk/330/3/ESMS.zip
• 21. https://archive.researchdata.leeds.ac.uk/330/3/ESMS.zip
• 22. https://archive.researchdata.leeds.ac.uk/330/3/ESMS.zip
• 23. https://archive.researchdata.leeds.ac.uk/330/4/crystal.zip
• 24. https://archive.researchdata.leeds.ac.uk/330/4/crystal.zip
• 25. https://archive.researchdata.leeds.ac.uk/330/4/crystal.zip
• 26. https://archive.researchdata.leeds.ac.uk/330/4/crystal.zip
• 27. https://archive.researchdata.leeds.ac.uk/330/5/XRPD.zip
• 28. https://archive.researchdata.leeds.ac.uk/330/5/XRPD.zip
• 29. https://archive.researchdata.leeds.ac.uk/330/5/XRPD.zip
• 30. https://archive.researchdata.leeds.ac.uk/330/5/XRPD.zip
• 31. https://archive.researchdata.leeds.ac.uk/330/6/NMR.zip
• 32. https://archive.researchdata.leeds.ac.uk/330/6/NMR.zip
• 33. https://archive.researchdata.leeds.ac.uk/330/6/NMR.zip
• 34. https://archive.researchdata.leeds.ac.uk/330/6/NMR.zip