Research Data Leeds Repository

Data to support study of silver(I) complexes of bis- and tris-(pyrazolyl)azine derivatives – dimers, coordination polymers and a pentametallic assembly

Halcrow, Malcolm A and Capel Berdiell, Izar and Warriner, Stuart L (2018) Data to support study of silver(I) complexes of bis- and tris-(pyrazolyl)azine derivatives – dimers, coordination polymers and a pentametallic assembly. University of Leeds. [Dataset] https://doi.org/10.5518/346

Dataset description

Two solvatomorphs of [Ag(tpt)]BF4·nMeNO2 (tpt = 2,4,6-tri{pyrazol-1-yl}pyridine) form face-to-face dimers linked by bridging pyrazolyl donors, or an unsupported chain-of-helicate dimers. Discrete silver dimers, coordination polymers and a pentanuclear cluster supported by related heterocyclic ligands are also described

Keywords:	silver; N-donor ligands; coordination polymers; X-ray crystallography
Subjects:	F000 - Physical sciences > F100 - Chemistry
Divisions:	Faculty of Engineering and Physical Sciences > School of Chemistry
Related resources:	Location Type https://doi.org/10.1039/C8DT00640G Publication http://eprints.whiterose.ac.uk/129258/ Publication
License:	Creative Commons Attribution 4.0 International (CC BY 4.0)
Date deposited:	16 Mar 2018 11:46
URI:	http://archive.researchdata.leeds.ac.uk/id/eprint/330
Additional details Additional details Creators: Creators ORCID Other ID Email Primary affiliation Primary affiliation ID Primary affiliation ID type Secondary affiliation Secondary affiliation ID Secondary affiliation ID type Halcrow, Malcolm A https://orcid.org/0000-0001-7491-9034 Capel Berdiell, Izar https://orcid.org/0000-0003-3828-7097 Warriner, Stuart L https://orcid.org/0000-0002-7589-6011 Type of data: Dataset Research funders: Leverhulme Trust Grant numbers: RPG-2015-095 Publication date: 2018 Resource language: English Research project title: Exploiting a spin-crossover module Publisher: University of Leeds Contact Email Address: m.a.halcrow@leeds.ac.uk Last Modified: 09 Jul 2018 13:45

Files

Documentation

compound naming and metadata [300kB] compound naming and metadata [300kB] compound naming and metadata [300kB] Visible to: Anyone File name: readme.pdf Content type: Documentation Mime-Type: application/pdf License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 300kB

Data

CHN microanalysis [2MB] CHN microanalysis [2MB] CHN microanalysis [2MB] Visible to: Anyone File name: Microanalyses.pdf Content type: Data Mime-Type: application/pdf License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 2MB

Mass spectrum [878kB] Mass spectrum [878kB] Mass spectrum [878kB] Visible to: Anyone File name: ESMS.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 878kB

Single crystal X-ray diffraction [2MB] Single crystal X-ray diffraction [2MB] Single crystal X-ray diffraction [2MB] Visible to: Anyone File name: crystal.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 2MB

X-ray powder diffraction [431kB] X-ray powder diffraction [431kB] X-ray powder diffraction [431kB] Visible to: Anyone File name: XRPD.zip Content type: Data Mime-Type: XRPD.zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 431kB

NMR spectra [1MB] NMR spectra [1MB] NMR spectra [1MB] Visible to: Anyone File name: NMR.zip Content type: Data Mime-Type: application/zip License: Creative Commons Attribution 4.0 International (CC BY 4.0) File size: 1MB